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myhra sverre; rivière john c. - characterization of nanostructures

Characterization of Nanostructures

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Dettagli

Genere:Libro
Lingua: Inglese
Editore:

CRC Press

Pubblicazione: 06/2012
Edizione: 1° edizione





Note Editore

The techniques and methods that can be applied to materials characterization on the microscale are numerous and well-established. Divided into two parts, Characterization of Nanostructures provides thumbnail sketches of the most widely used techniques and methods that apply to nanostructures, and discusses typical applications to single nanoscale objects, as well as to ensembles of such objects. Section I: Techniques and Methods overviews the physical principles of the main techniques and describes those operational modes that are most relevant to nanoscale characterization. It provides sufficient technical detail so that readers and prospective users can gain an appreciation of the strengths and limitations of particular techniques. The section covers both mainstream and less commonly used techniques. Section II: Applications of Techniques to Structures of Different Dimensionalities and Functionalities deals with the methods for materials characterization of generic types of systems, using carefully chosen illustrations from the literature. Each chapter begins with a brief description of the materials and supplies a context for the methods for characterization. The volume concludes with a series of flow charts and brief descriptions of tactical issues. The authors focus on the needs of the research laboratory but also address those of quality control, industrial troubleshooting, and online analysis. Characterization of Nanostructures describes those techniques and their operational modes that are most relevant to nanoscale characterization. It is especially relevant to systems of different dimensionalities and functionalities. The book builds a bridge between generalists, who play vital roles in the post-disciplinary area of nanotechnology, and specialists, who view themselves as more in the context of the discipline.




Sommario

Introduction to Characterization of NanostructuresNanotechnology—In the Beginning There Was the IdeaNanotechnology as a Practical PropositionWhat Is Nanotechnology?Materials Characterization—What Is It?Current State of ‘Best Practice’ and QASection I Techniques and MethodsElectron-Optical Imaging of Nanostructures ((HR)TEM, STEM, and SEM)IntroductionTEM OverviewInteractions of Electrons with MatterAberration CorrectionScanning Transmission Electron Microscopy (STEM)The Issue of Radiation Damage during Imaging and Analysis Examples of SEM PerformanceOptimization of Image QualityElectron-Optical Analytical TechniquesIntroductionLoss ProcessesEDSEELSTechnical Implementation and MethodsComplementarity of EDS and EELS: A Case StudyPhoton-Optical Spectroscopy—Raman and FluorescenceIntroductionRaman SpectroscopyFluorescence SpectroscopyScanning Probe Techniques and MethodsIntroductionTechnical ImplementationSTM/STSSFMSCMSNOMSECMScanning Kelvin Probe (SKP)Scanning Ion Current Microscopy (SICM)Future ProspectsTechniques and Methods for Nanoscale Analysis of Single Particles and Ensembles of ParticlesIntroductionPhoton-Correlation Spectroscopy (PCS) or Dynamic Light Scattering (DLS)Differential Centrifugal Sedimentation (DCS)Zeta PotentialDifferential Mobility Spectrometry (DMS)Surface Area DeterminationSurface and Bulk ChemistryOverview—Choices of Technique(s)Section II ApplicationsC60 and Other Cage StructuresIntroductionCharacterization of Fullerenes and FullereneCompoundsEndohedral FullerenesFullerites Peapod Fullerenes in CNTQuantum Dots and Related StructuresIntroductionParticles in 2-D and 3-D ConfinementSynthesis Routes for Quantum DotsCharacterization of Quantum DotsAbsorption and Photoluminescence Spectroscopy of Quantum DotsCarbon Nanotubes and Other Tube StructuresIntroductionDescription of CNT StructureSynthesis RoutesElectronic Structure of Graphene and SWCNTGeneral Characteristics of CNTsOther Tube StructuresCharacterization of NanotubesNanowiresIntroductionSynthesis RoutesCharacterisation of Nanowires by SEM and TEMCharacterisation of Nanowire HeterostructuresCharacterization Related to Potential ApplicationsGraphene and Other Monolayer StructuresIntroductionGraphene StructureSummary of Electronic StructureOther 2-D Structures (Nanosheets)Overview of Synthesis RoutesStructural CharacterizationRaman Spectroscopic CharacterizationCharacterization of Electronic StructureNanostructures—Strategic and Tactical IssuesThinking about StrategyThinking about TacticsStrategic IssuesPreparation of Specimens for Characterization of NanostructuresEnsemble Averages: Limitations‘Soft’ Materials—Specimen PreparationCleanlinessUser-friendlinessCost-Effectiveness




Autore

Sverre Myhra and John Riviere are affiliated with Oxford University, UK.










Altre Informazioni

ISBN:

9781439854150

Condizione: Nuovo
Dimensioni: 9.25 x 6.25 in Ø 1.85 lb
Formato: Copertina rigida
Illustration Notes:228 b/w images, 25 color images, 16 tables and 25 color figures/16 page insert follows page 76
Pagine Arabe: 350


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